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@ARTICLE{Haslbeck:137990,
author = {Haslbeck, Veronika and Drazic, Adrian and Eckl, Julia M and
Alte, Ferdinand and Helmuth, Martin and Popowicz, Grzegorz
and Schmidt, Werner and Braun, Frank and Weiwad, Matthias
and Fischer, Gunter and Gemmecker, Gerd and Sattler, Michael
and Striggow, Frank and Groll, Michael and Richter, Klaus},
title = {{S}elective activators of protein phosphatase 5 target the
auto-inhibitory mechanism.},
journal = {Bioscience reports},
volume = {35},
number = {3},
issn = {0144-8463},
address = {Colchester},
publisher = {Portland Press},
reportid = {DZNE-2020-04312},
pages = {e00210},
year = {2015},
abstract = {Protein phosphatase 5 (PP5) is an evolutionary conserved
serine/threonine phosphatase. Its dephosphorylation activity
modulates a diverse set of cellular factors including
protein kinases and the microtubule-associated tau protein
involved in neurodegenerative disorders. It is
auto-regulated by its heat-shock protein (Hsp90)-interacting
tetratricopeptide repeat (TPR) domain and its C-terminal
α-helix. In the present study, we report the identification
of five specific PP5 activators [PP5 small-molecule
activators (P5SAs)] that enhance the phosphatase activity up
to 8-fold. The compounds are allosteric modulators
accelerating efficiently the turnover rate of PP5, but do
barely affect substrate binding or the interaction between
PP5 and the chaperone Hsp90. Enzymatic studies imply that
the compounds bind to the phosphatase domain of PP5. For the
most promising compound crystallographic comparisons of the
apo PP5 and the PP5-P5SA-2 complex indicate a relaxation of
the auto-inhibited state of PP5. Residual electron density
and mutation analyses in PP5 suggest activator binding to a
pocket in the phosphatase/TPR domain interface, which may
exert regulatory functions. These compounds thus may expose
regulatory mechanisms in the PP5 enzyme and serve to develop
optimized activators based on these scaffolds.},
keywords = {Animals / Caenorhabditis elegans Proteins: metabolism /
Crystallography, X-Ray / Drug Evaluation, Preclinical:
methods / Enzyme Activation: drug effects / HSC70 Heat-Shock
Proteins: genetics / HSC70 Heat-Shock Proteins: metabolism /
Mutation / Nuclear Magnetic Resonance, Biomolecular /
Nuclear Proteins: antagonists $\&$ inhibitors / Nuclear
Proteins: chemistry / Nuclear Proteins: metabolism /
Phosphoprotein Phosphatases: antagonists $\&$ inhibitors /
Phosphoprotein Phosphatases: chemistry / Phosphoprotein
Phosphatases: metabolism / Protein Domains / Rats / Small
Molecule Libraries: pharmacology / Caenorhabditis elegans
Proteins (NLM Chemicals) / HSC70 Heat-Shock Proteins (NLM
Chemicals) / Nuclear Proteins (NLM Chemicals) / Small
Molecule Libraries (NLM Chemicals) / Phosphoprotein
Phosphatases (NLM Chemicals) / protein phosphatase 5 (NLM
Chemicals)},
cin = {AG Striggow},
ddc = {540},
cid = {I:(DE-2719)5000045},
pnm = {342 - Disease Mechanisms and Model Systems (POF3-342)},
pid = {G:(DE-HGF)POF3-342},
typ = {PUB:(DE-HGF)16},
pubmed = {pmid:26182372},
pmc = {pmc:PMC4721540},
doi = {10.1042/BSR20150042},
url = {https://pub.dzne.de/record/137990},
}